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Research Article

E-J.Chem , Volume 4, Number 2, p 265-271

Synthesis, Characterization and Copolymerization of
N-(phenylamino)maleimide with MMA


B. L. HIRAN, S. N. PALIWAL, JYOTI CHOUDHARY
and P. R. CHOUDHARY

Chemical Kinetics and Polymer Research Laboratory, Department of Chemistry,
M. L. S. University, Udaipur (Raj.) India.313 001.

ABSTRACT

The free radical copolymerization of N-(phenylamino)maleimide (NPAMI) was carried. The copolymerization with methyl methacrylate (MMA) was performed at 65°C with AIBN as the initiator in THF solvent. Resulting copolymer was characterized by density measurement, intrinsic viscosity, solubility, FT-IR & 1H NMR spectroscopy. Effect of the solvent and time on copolymer yield was also investigated. The molecular weight of copolymer was determined by gel permeation chromatography (GPC). The thermal stability of copolymer was determined by Thermogravimetric analysis (TGA).

Received 23 November 2006; Accepted 22 December 2006

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Corresponding Author

B. L. HIRAN
Chemical Kinetics and Polymer Research Laboratory,
Department of Chemistry,
M. L. S. University,
Udaipur (Raj.) -313 001.
India.
hiranbl@rediffmail.com

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