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Research Article

E-J.Chem , Volume 4, Number 2, p 199-207

Synthesis and Thermal Degradation Kinetics of Co(II), Ni(II),
Cd(II), Zn(II), Pd(II), Rh(III) and Ru(III) Complexes with Methylquinolino[3,2-b]benzodiazepine


BENNEHALLI BASAVARAJU and HALEHATTI S. BHOJYA NAIK

Department of Biotechnology, GM Institute of Technology, Davangere-577 006, Karnataka, India.
Department of PG studies and Research in Industrial Chemistry, School of Chemical Sciences, Kuvempu University, Shankaraghatta-577451, Shimoga, Karnataka, India.

ABSTRACT

A series of new complexes formed by the interaction of a new ligand Methylquinolino[3,2-b]benzodiazepine (L) with various transition metal ions have been isolated and characterized by elemental analysis and electronic, IR, magnetic moment and conductivity measurements. Thermogravimetric (TG) studies of the complexes have been performed in order to establish the mode of their thermal degradation. The thermal degradation was found to proceed in two steps. The kinetics and thermodynamic parameters were computed from the thermal decomposition data.


Received 3 October 2006; Accepted 1 November 2006

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Corresponding Author

BENNEHALLI BASAVARAJU
Department of Biotechnology,
GM Institute of Technology,
Davangere-577 006, Karnataka,
India.
basavaraju_b@yahoo.co.in



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